عنوان

Solid-State NMR in zeolite catalysis /

(Number (ISBN

9789811369650

(Number (ISBN

9789811369667

(Number (ISBN

9789811369674

(Number (ISBN

9811369658

(Number (ISBN

9811369666

(Number (ISBN

9811369674

Erroneous ISBN

9789811369650

Title Proper

Solid-State NMR in zeolite catalysis /

General Material Designation

[Book]

First Statement of Responsibility

Jun Xu, Qiang Wang, Shenhui Li and Feng Deng.

Place of Publication, Distribution, etc.

Singapore :

Name of Publisher, Distributor, etc.

Springer,

Date of Publication, Distribution, etc.

[2019]

Date of Publication, Distribution, etc.

©2019

Specific Material Designation and Extent of Item

1 online resource

Series Title

Lecture notes in chemistry ;

Volume Designation

Volume 103

Text of Note

Includes bibliographical references and index.

Text of Note

Intro; Preface; Contents; 1 Solid-State NMR Principles and Techniques; 1.1 Introduction; 1.2 Nuclear Spin Interactions in Solids; 1.2.1 Chemical Shift Interaction; 1.2.2 Dipole-Dipole Interaction; 1.2.3 Quadrupolar Interaction; 1.2.4 Spin-Spin Interaction; 1.3 Manipulations of Spin Interactions in Solids; 1.3.1 Magic-Angle Spinning (MAS); 1.3.2 Cross-Polarization; 1.3.3 Dipolar Decoupling Methods in Rotating Solid; 1.3.4 Dipolar Recoupling Methods in Rotating Solid; 1.3.5 High-Resolution Techniques for Half-Integer-Spin Quadrupolar Nuclei; 1.3.6 Summary; References

Text of Note

2 Solid-State NMR Studies of Zeolites and Zeotype Materials Synthesis2.1 Introduction; 2.2 Zeolite Synthesis Route and Procedures; 2.3 Zeolite Synthesis Process and Crystallization Mechanism; 2.4 NMR Strategy in Characterization of Zeolite Synthesis; 2.4.1 Microporous Aluminosilicates; 2.4.2 Microporous Aluminophosphates; 2.5 Summary; References; 3 Solid-State NMR Characterization of Framework Structure of Zeolites and Zeotype Materials; 3.1 Introduction; 3.2 Solid-State NMR Characterization of Zeolite Framework Structure; 3.2.1 27Al MAS NMR; 3.2.2 29Si MAS NMR; 3.2.3 31P MAS NMR

Text of Note

3.2.4 17O MAS NMR3.2.5 129Xe NMR; 3.2.6 Other Framework Elements; 3.3 Summary; References; 4 Solid-State NMR Characterization of Host-Guest Interactions; 4.1 Introduction; 4.2 Solid-State NMR Characterization of Host-Guest Interactions; 4.2.1 Host-Guest Interaction Between Adsorbed Molecule and Zeolite Framework; 4.2.2 Host-Guest Interaction in Molecular Sieve Synthesis; 4.2.3 Host-Guest Interaction in Zeolite Catalysis; 4.3 Summary; References; 5 Solid-State NMR Characterization of Acid Properties of Zeolites and Solid Acid Catalysts; 5.1 Introduction

Text of Note

5.2 Solid-State NMR Characterization of Acidic Property5.2.1 Acid Sites Containing Hydroxyl Groups; 5.2.2 Acidic Nature and Strength; 5.2.3 Location and Distribution of Acid Sites; 5.2.4 Spatial Proximities and Synergy Effects of Different Acid Sites; 5.3 Summary; References; 6 In Situ Solid-State NMR Investigation of Catalytic Reactions on Zeolites; 6.1 Introduction; 6.2 In Situ Solid-State NMR Approaches; 6.2.1 Batch Reaction; 6.2.2 Flow Reaction; 6.3 Mechanistic Study of the Catalytic Reactions by In Situ NMR; 6.3.1 Activation and Conversion of Light Alkanes

Text of Note

6.3.2 Methanol-to-Olefins (MTO) Conversion6.4 Summary; References; Index

0

8

8

8

8

Text of Note

Solid-State NMR Characterization of Heterogeneous Catalysts and Catalytic Reactions provides a comprehensive account of state-of-the-art solid-state NMR techniques and the application of these techniques in heterogeneous catalysts and related catalytic reactions. It includes an introduction to the basic theory of solid-state NMR and various frequently used techniques. Special emphasis is placed on characterizing the framework and pore structure, active site, guest-host interaction, and synthesis mechanisms of heterogeneous catalysts using multinuclear one- and two-dimensional solid-sate NMR spectroscopy. Additionally, various in-situ solid-state NMR techniques and their applications in investigation of the mechanism of industrially important catalytic reactions are also discussed. Both the fundamentals and the latest research results are covered, making the book suitable as a reference guide for both experienced researchers in and newcomers to this field. Feng Deng is a Professor at Wuhan Institute of Physics and Mathematics, Chinese Academy of Sciences.

Source for Acquisition/Subscription Address

Springer Nature

Stock Number

com.springer.onix.9789811369674

International Standard Book Number

9789811369650

International Standard Book Number

9789811369667

Nuclear magnetic resonance spectroscopy.

Zeolite catalysts.

BUSINESS & ECONOMICS-- Industries-- General.

Nuclear magnetic resonance spectroscopy.

Zeolite catalysts.

BUS-- 070000

PNRD

PNRD

Number

Edition

Class number

Xu, Jun

Deng, Feng

Li, Shenhui

Wang, Qiang

Date of Transaction

20200823232946.0

Cataloguing Rules (Descriptive Conventions))

pn

Electronic name

[Book]

Y