Optimizing NMR methods for structure elucidation :
نام عام مواد
[Book]
ساير اطلاعات عنواني
characterizing natural products and other organic compounds /
نام نخستين پديدآور
Darcy C. Burns, William F. Reynolds.
وضعیت نشر و پخش و غیره
محل نشرو پخش و غیره
[Cambridge] :
نام ناشر، پخش کننده و غيره
Royal Society of Chemistry,
تاریخ نشرو بخش و غیره
2018.
مشخصات ظاهری
نام خاص و کميت اثر
1 online resource
فروست
عنوان فروست
New developments in NMR ;
مشخصه جلد
17
يادداشت کلی
متن يادداشت
Includes index.
متن يادداشت
Title from title details screen.
یادداشتهای مربوط به مندرجات
متن يادداشت
Cover; Author Biographies; Acknowledgements; Dedication; Contents; Chapter 1 Introduction; References; Chapter 2 Basics of the NMR Experiment; 2.1 Spin and Magnetic Properties of Nuclei; 2.2 Behavior of Magnetic Nuclei in a Static External Magnetic Field; 2.3 Alternative Simplified Descriptions of the Basic NMR Experiment; 2.4 Key NMR Parameters; 2.4.1 Chemical Shifts; 2.4.2 Coupling Constants; 2.4.3 Relaxation Times; 2.4.4 Nuclear Overhauser Enhancements; References; Chapter 3 Pulsed Fourier Transform NMR; 3.1 Historical Background; 3.2 Basic Theory of Pulsed FT NMR.
متن يادداشت
3.3 Sampling Rate, Dwell Time, Acquisition Time and Digital Resolution3.4 Analog to Digital Conversion and Digital Oversampling; 3.5 Quadrature Detection; 3.6 Fold-in Peaks and Analog or Digital Filters; 3.7 Avoiding Partial Saturation in Multi-scan Spectra; 3.8 Zero Filling; References; Chapter 4 The NMR Spectrometer; 4.1 The Magnet; 4.1.1 Superconducting Solenoids; 4.1.2 Potential Future Developments; 4.2 NMR Probes; 4.2.1 Room Temperature Probes; 4.2.2 Cryogenically Cooled Probes; 4.2.3 Flow NMR Probes; 4.3 Console; 4.4 Other Useful Accessories; 4.5 Buying an NMR Spectrometer.
متن يادداشت
4.6 Maintaining an NMR SpectrometerReferences; Chapter 5 Acquiring 1H and 13C Spectra; 5.1 1H and 13C Spin-Lattice Relaxation Times for Typical Organic Molecules in the 150-450 Dalton Molecular Weight Range; 5.2 Sample and Spectrometer Preparation; 5.2.1 Solvent Choice; 5.2.2 Sample Preparation; 5.2.3 Spectrometer Preparation; 5.3 Acquiring and Processing Routine 1H Spectra; 5.4 Acquiring and Processing Routine 13C Spectra; 5.5 Reporting Data for Routine 1H and 3C Spectra; 5.6 Acquiring Quantitative 1H Spectra; 5.6.1 Reasons for Acquiring Quantitative 1H NMR Spectra.
متن يادداشت
5.6.2 Conditions for Acquiring Quantitative Spectra and Accurately Measuring Peak Areas5.6.3 Internal Versus External Referencing; 5.7 Summary of Recommendations for Chapter 5; References; Chapter 6 One-dimensional Pulse Sequences; 6.1 Relaxation Time Measurements; 6.1.1 T1 Measurements; 6.1.2 T2 Measurements; 6.2 Pulse Sequences for 13C Spectral Editing; 6.2.1 INEPT and DEPT; 6.2.2 APT and CRAPT; 6.3 Pulse Sequences for Solvent Suppression; 6.4 Pure Shift Pulse Sequences; References; Chapter 7 Two-dimensional NMR Basics.
متن يادداشت
7.1 Alternative Methods of Generating Information During the Evolution Period7.2 Homonuclear or Heteronuclear 2D Spectra; 7.3 Direct Detection or Inverse Detection for Heteronuclear 2D Sequences; 7.4 Absolute Value or Phase Sensitive 2D Spectra; 7.5 Weighting Functions for Processing 2D Data Sets; 7.6 Coherence Pathways, Phase Cycling and Gradient Selection; 7.6.1 Coherence Pathways; 7.6.2 Phase Cycling; 7.6.3 Gradient Selection; 7.7 Alternative Acquisition and Processing Methods for Saving Time When Acquiring 2D Spectra; 7.7.1 Forward Linear Prediction; 7.7.2 Non-uniform (Sparse) Sampling.
بدون عنوان
0
بدون عنوان
8
بدون عنوان
8
بدون عنوان
8
بدون عنوان
8
یادداشتهای مربوط به خلاصه یا چکیده
متن يادداشت
This book is aimed at informing organic chemists and natural products chemists on the use of NMR for structure elucidation to enable them to ensure they yield the most reliable possible data in the minimum possible time.
یادداشتهای مربوط به سفارشات
منبع سفارش / آدرس اشتراک
Ingram Content Group
شماره انبار
3-178-9781788010498
ویراست دیگر از اثر در قالب دیگر رسانه
شماره استاندارد بين المللي کتاب و موسيقي
9781782625391
موضوع (اسم عام یاعبارت اسمی عام)
موضوع مستند نشده
Natural products-- Spectra.
موضوع مستند نشده
Nuclear magnetic resonance.
موضوع مستند نشده
Organic compounds-- Spectra.
موضوع مستند نشده
Natural products-- Spectra.
موضوع مستند نشده
Nuclear magnetic resonance.
موضوع مستند نشده
Organic chemistry.
موضوع مستند نشده
Organic compounds-- Spectra.
موضوع مستند نشده
SCIENCE-- Chemistry-- Organic.
موضوع مستند نشده
Scientific equipment, experiments & techniques.
مقوله موضوعی
موضوع مستند نشده
PDN
موضوع مستند نشده
PNN
موضوع مستند نشده
SCI-- 013040
رده بندی ديویی
شماره
547
.
046
ويراست
23
رده بندی کنگره
شماره رده
QC462
.
5
نام شخص به منزله سر شناسه - (مسئولیت معنوی درجه اول )