Novel synthesis of vegetable oil derived corrosion inhibitors
نام عام مواد
[Thesis]
نام نخستين پديدآور
Sonia Joseph Hanna Kasshanna
نام ساير پديدآوران
Rostron, Paul
وضعیت نشر و پخش و غیره
نام ناشر، پخش کننده و غيره
The Petroleum Institute (United Arab Emirates)
تاریخ نشرو بخش و غیره
2016
مشخصات ظاهری
نام خاص و کميت اثر
108
يادداشت کلی
متن يادداشت
Committee members: El Kadi, Mirella; Vukusic, Sulafudin
یادداشتهای مربوط به نشر، بخش و غیره
متن يادداشت
Place of publication: United States, Ann Arbor; ISBN=978-1-369-37463-6
یادداشتهای مربوط به پایان نامه ها
جزئيات پايان نامه و نوع درجه آن
M.S.
نظم درجات
Applied Chemistry
کسي که مدرک را اعطا کرده
The Petroleum Institute (United Arab Emirates)
امتياز متن
2016
یادداشتهای مربوط به خلاصه یا چکیده
متن يادداشت
This thesis has been able to examine a novel one-pot synthesis of fatty acid amides which is derived from natural vegetable oil. The sodium methoxide was used to esterify a series of natural products of vegetable oil, which include: linseed oil, sunflower oil, peanut oil, cress oil, almond oil and canola oil. The mixture was refluxed for 1 hour at 90 °C under N 2 gas atmosphere in order to produce methylester. Then, a concentrated aqueous ammonia solution was added to the product of the first step reaction and refluxed for 3 hours at 150 °C with no N2 gas to form a fatty acid amide. The progress of the reaction was qualitatively followed using a Thin Layer Chromatography (TLC) technique with ethyl acetate as eluent. TLC plates at which spots of each of the vegetable oil, methylester and amide were placed and then investigated using UV lamp. Fourier Transform Infrared Spectroscopy (FTIR) was used to investigate the different samples of the reaction mixture in order to determine the functional group transformation between the starting material and the final product. Both TLC and FTIR techniques were successful and showed respectively, different migration rates and functional group transformation.