3.3 Choice of a Rotor Type3.3.1 Classification of Centrifuge Rotors; 3.3.1.1 Fixed-Angle Rotors; 3.3.1.2 Swing-Out Rotors; 3.3.1.3 Zonal Rotors; 3.3.1.4 Vertical Rotors; 3.3.2 The Selection Principle of the Rotors; 3.3.3 The Relationship Between the Type of the Rotor and Centrifugal Force; 3.3.3.1 Centrifugal Force; 3.3.3.2 Relative Centrifugal Force (RCF); 3.3.3.3 The Selection of Speed (N) and Relative Centrifugal Force (RCF); 3.4 Choice of an Appropriate Separation Speed and Time; 3.4.1 Differential Centrifugation; 3.4.2 Isopycnic Centrifugation; 3.4.3 Rate-Zonal Centrifugation.
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Appendix: MATLAB Program for the Computational Mathematical Optimization of Spherical NanoparticlesReferences; 5 Density Gradient Ultracentrifugation of Colloidal Nanostructures; Abstract; 5.1 Separation of Zero-Dimensional Nanostructures; 5.2 Separation of One-Dimensional Nanostructures; 5.3 Separation of Two-Dimensional Nanostructures; 5.4 Separation of Assemblies/Clusters; References; 6 Application of Nanoseparation in Reaction Mechanism Analysis; Abstract; 6.1 The Concept of "lab in a tube"; 6.2 Size-Property Investigation Through DGUC Nanoseparation.
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SUMMARY OR ABSTRACT
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This brief introduces the classification and mechanism of density gradient ultracentrifugation (DGUC) method with rich examples showing the versatility of such an efficient separation technique. It also gives a strict mathematical description and a computational optimization model to predict the best separation parameters for a given colloidal system. The concept of "Lab in a tube" is proposed in the last chapter, which allows the size-property relationship investigation, synthetic optimization and reaction/assembly mechanism exploration etc.
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9789811051890
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Title
Nanoseparation using density gradient ultracentrifugation.