عنوان
پدید آورنده
موضوع
رده
QD117.C517 G74 2019
QD117
.
C517
G74
2019
کتابخانه
محل استقرار
INTERNATIONAL STANDARD BOOK NUMBER
(Number (ISBN
3030106500
(Number (ISBN
3030106519
(Number (ISBN
9783030106508
(Number (ISBN
9783030106515
Erroneous ISBN
3030106497
Erroneous ISBN
9783030106492
Erroneous ISBN
9783030106515
TITLE AND STATEMENT OF RESPONSIBILITY
Title Proper
Thermal field-flow fractionation of polymers /
General Material Designation
[Book]
First Statement of Responsibility
Guilaume Greyling, Harald Pasch.
.PUBLICATION, DISTRIBUTION, ETC
Place of Publication, Distribution, etc.
Cham, Switzerland :
Name of Publisher, Distributor, etc.
Springer,
Date of Publication, Distribution, etc.
[2019]
PHYSICAL DESCRIPTION
Specific Material Designation and Extent of Item
1 online resource
SERIES
Series Title
Springer Laboratory Manuals in polymer science
INTERNAL BIBLIOGRAPHIES/INDEXES NOTE
Text of Note
Includes bibliographical references and index.
CONTENTS NOTE
Text of Note
Intro; Preface; Contents; Symbols and Abbreviations; 1: Introduction; 1.1 The Complex Nature of Polymers; 1.2 Column-Based Liquid Chromatography of Polymers; 1.3 Field-Flow Fractionation; 1.3.1 Mechanism of FFF; 1.3.2 Subtechniques of Field-Flow Fractionation; References; 2: Thermal Field-Flow Fractionation (ThFFF); 2.1 Thermal Field-Flow Fractionation as a Powerful Alternative to Column-Based Liquid Chromatography; 2.2 Thermal Diffusion of Polymers; 2.3 Carrier Liquid Characteristics; 2.3.1 Aqueous Carrier Liquids; 2.3.2 Carrier Liquid Viscosity; 2.3.3 Polymer Solubility
Text of Note
2.3.3.1 Good Solvents2.3.3.2 Poor Solvents; 2.3.3.3 Theta Solvent; 2.3.4 Carrier Liquid Polarity; 2.3.5 Binary Solvent Carrier Liquids and Thermal Diffusion; 2.4 Determining Chemical Composition from ThFFF; 2.5 Recent Advances and Applications; 2.5.1 ThFFF with Organic Carrier Liquids; 2.5.2 ThFFF with Aqueous Carrier Liquids; References; 3: Applications and Experimental Design; 3.1 Instrumentation; 3.1.1 ThFFF; 3.1.2 Detection; 3.1.2.1 Differential Refractive Index Detection (dRI); 3.1.2.2 Dynamic Light Scattering Detector (DLS); 3.1.2.3 Multiangle Laser Light Scattering Detection (MALLS)
Text of Note
3.1.3 1H NMR Spectroscopy3.2 Example 1: Chemical Composition of Block Copolymers; 3.2.1 Characterisation of Polystyrene-poly(butyl acrylate) and Polystyrene-poly(methyl acrylate) Diblock Copolymers [5, 6]; 3.2.2 Characterization of Polystyrene-poly(t-butyl acrylate)-poly(methyl methacrylate) Linear Triblock Copolymer [6]; 3.3 Example 2: Microstructure Analysis; 3.3.1 Polybutadiene and Polyisoprene [18]; 3.3.2 Isotactic and Syndiotactic Poly(methyl methacrylate) [17]; 3.3.3 Poly(n-butyl methacrylate) and Poly(t-butyl methacrylate) [19]; 3.4 Example 3: Solvent Partitioning [29]
Text of Note
3.5 Example 4: Self-Assemblies in Organic Carrier Liquids3.5.1 Characterisation of PB-PS Micelles According to Corona Composition [49]; 3.5.2 Characterisation of PB-PS Micelles According to Core Composition [54]; 3.5.3 Characterisation of PS-PEO Self-Assemblies According to Morphology [60]; 3.6 Example 5: Aqueous ThFFF; 3.6.1 Poly(methacrylic acid) and Poly(vinyl pyridine) [78]; 3.6.1.1 Isotactic and Syndiotactic PMAA; 3.6.1.2 Poly(4-vinyl pyridine) and Poly(2-vinyl pyridine); 3.6.2 Cationic and Anionic Charged Self-Assemblies [79]; 3.6.2.1 PMAA-PMMA Micelles
Text of Note
3.6.2.2 P2VP-PS and P4VP-PS MicellesReferences; 4: Conclusions and Future Trends; 5: Troubleshooting; 5.1 Spacer and Temperature Drop; 5.2 Cold Wall Temperature; 5.3 Carrier Liquid; 5.3.1 Type of Analyte; 5.3.2 Convenience; 5.3.3 Physical Properties; 5.3.4 Carrier Liquid Composition; 5.4 Determining Diffusion Coefficients for Complex Samples; 5.5 Poor Resolution; 5.6 Low Solute Recovery and Peak Shape; 5.7 Relaxation Time and Flow Rate Effects; 5.8 Overloading; 5.9 Sample Preparation; 5.10 Excessively High Pressure; 5.10.1 High Pump Pressure; 5.10.2 High Channel Pressure; 5.10.3 Detectors
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SUMMARY OR ABSTRACT
Text of Note
This book introduces the reader to thermal field-flow fractionation and discusses its advantages over the fundamental problems associated with traditional column-based analytical techniques commonly used to characterize polymers and macromolecules. The authors discuss the theoretical background, equipment, experimental procedures as well as the recent advances and applications of thermal field-flow fractionation. Complete with several practical examples and troubleshooting guidelines, the book is written for beginners and experienced separation scientists alike and will enable its readers to optimize their experimental conditions for their specific separation needs and problems.
ACQUISITION INFORMATION NOTE
Source for Acquisition/Subscription Address
Springer Nature
Stock Number
com.springer.onix.9783030106508
OTHER EDITION IN ANOTHER MEDIUM
Title
Thermal field-flow fractionation of polymers.
International Standard Book Number
9783030106492
TOPICAL NAME USED AS SUBJECT
Field-flow fractionation.
Membrane separation.
Polymers-- Analysis.
Field-flow fractionation.
Membrane separation.
Polymers-- Analysis.
SCIENCE-- Chemistry-- Analytic.
(SUBJECT CATEGORY (Provisional
PNNP
PNNP
SCI-- 013010
DEWEY DECIMAL CLASSIFICATION
Number
543/
.
84
Edition
23
LIBRARY OF CONGRESS CLASSIFICATION
Class number
QD117
.
C517
Book number
G74
2019
PERSONAL NAME - PRIMARY RESPONSIBILITY
Greyling, Guilaume
PERSONAL NAME - ALTERNATIVE RESPONSIBILITY
Pasch, Harald,1952-
ORIGINATING SOURCE
Date of Transaction
20200823082440.0
Cataloguing Rules (Descriptive Conventions))
pn
ELECTRONIC LOCATION AND ACCESS
Electronic name
مطالعه متن کتاب [Book]
Y
