عنوان
پدید آورنده
موضوع
رده
QC462.5
QC462
.
5
کتابخانه
محل استقرار
INTERNATIONAL STANDARD BOOK NUMBER
(Number (ISBN
1788010493
(Number (ISBN
1788015355
(Number (ISBN
9781788010498
(Number (ISBN
9781788015356
Erroneous ISBN
1782625399
Erroneous ISBN
9781782625391
TITLE AND STATEMENT OF RESPONSIBILITY
Title Proper
Optimizing NMR methods for structure elucidation :
General Material Designation
[Book]
Other Title Information
characterizing natural products and other organic compounds /
First Statement of Responsibility
Darcy C. Burns, William F. Reynolds.
.PUBLICATION, DISTRIBUTION, ETC
Place of Publication, Distribution, etc.
[Cambridge] :
Name of Publisher, Distributor, etc.
Royal Society of Chemistry,
Date of Publication, Distribution, etc.
2018.
PHYSICAL DESCRIPTION
Specific Material Designation and Extent of Item
1 online resource
SERIES
Series Title
New developments in NMR ;
Volume Designation
17
GENERAL NOTES
Text of Note
Includes index.
Text of Note
Title from title details screen.
CONTENTS NOTE
Text of Note
Cover; Author Biographies; Acknowledgements; Dedication; Contents; Chapter 1 Introduction; References; Chapter 2 Basics of the NMR Experiment; 2.1 Spin and Magnetic Properties of Nuclei; 2.2 Behavior of Magnetic Nuclei in a Static External Magnetic Field; 2.3 Alternative Simplified Descriptions of the Basic NMR Experiment; 2.4 Key NMR Parameters; 2.4.1 Chemical Shifts; 2.4.2 Coupling Constants; 2.4.3 Relaxation Times; 2.4.4 Nuclear Overhauser Enhancements; References; Chapter 3 Pulsed Fourier Transform NMR; 3.1 Historical Background; 3.2 Basic Theory of Pulsed FT NMR.
Text of Note
3.3 Sampling Rate, Dwell Time, Acquisition Time and Digital Resolution3.4 Analog to Digital Conversion and Digital Oversampling; 3.5 Quadrature Detection; 3.6 Fold-in Peaks and Analog or Digital Filters; 3.7 Avoiding Partial Saturation in Multi-scan Spectra; 3.8 Zero Filling; References; Chapter 4 The NMR Spectrometer; 4.1 The Magnet; 4.1.1 Superconducting Solenoids; 4.1.2 Potential Future Developments; 4.2 NMR Probes; 4.2.1 Room Temperature Probes; 4.2.2 Cryogenically Cooled Probes; 4.2.3 Flow NMR Probes; 4.3 Console; 4.4 Other Useful Accessories; 4.5 Buying an NMR Spectrometer.
Text of Note
4.6 Maintaining an NMR SpectrometerReferences; Chapter 5 Acquiring 1H and 13C Spectra; 5.1 1H and 13C Spin-Lattice Relaxation Times for Typical Organic Molecules in the 150-450 Dalton Molecular Weight Range; 5.2 Sample and Spectrometer Preparation; 5.2.1 Solvent Choice; 5.2.2 Sample Preparation; 5.2.3 Spectrometer Preparation; 5.3 Acquiring and Processing Routine 1H Spectra; 5.4 Acquiring and Processing Routine 13C Spectra; 5.5 Reporting Data for Routine 1H and 3C Spectra; 5.6 Acquiring Quantitative 1H Spectra; 5.6.1 Reasons for Acquiring Quantitative 1H NMR Spectra.
Text of Note
5.6.2 Conditions for Acquiring Quantitative Spectra and Accurately Measuring Peak Areas5.6.3 Internal Versus External Referencing; 5.7 Summary of Recommendations for Chapter 5; References; Chapter 6 One-dimensional Pulse Sequences; 6.1 Relaxation Time Measurements; 6.1.1 T1 Measurements; 6.1.2 T2 Measurements; 6.2 Pulse Sequences for 13C Spectral Editing; 6.2.1 INEPT and DEPT; 6.2.2 APT and CRAPT; 6.3 Pulse Sequences for Solvent Suppression; 6.4 Pure Shift Pulse Sequences; References; Chapter 7 Two-dimensional NMR Basics.
Text of Note
7.1 Alternative Methods of Generating Information During the Evolution Period7.2 Homonuclear or Heteronuclear 2D Spectra; 7.3 Direct Detection or Inverse Detection for Heteronuclear 2D Sequences; 7.4 Absolute Value or Phase Sensitive 2D Spectra; 7.5 Weighting Functions for Processing 2D Data Sets; 7.6 Coherence Pathways, Phase Cycling and Gradient Selection; 7.6.1 Coherence Pathways; 7.6.2 Phase Cycling; 7.6.3 Gradient Selection; 7.7 Alternative Acquisition and Processing Methods for Saving Time When Acquiring 2D Spectra; 7.7.1 Forward Linear Prediction; 7.7.2 Non-uniform (Sparse) Sampling.
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8
8
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SUMMARY OR ABSTRACT
Text of Note
This book is aimed at informing organic chemists and natural products chemists on the use of NMR for structure elucidation to enable them to ensure they yield the most reliable possible data in the minimum possible time.
ACQUISITION INFORMATION NOTE
Source for Acquisition/Subscription Address
Ingram Content Group
Stock Number
3-178-9781788010498
OTHER EDITION IN ANOTHER MEDIUM
International Standard Book Number
9781782625391
TOPICAL NAME USED AS SUBJECT
Natural products-- Spectra.
Nuclear magnetic resonance.
Organic compounds-- Spectra.
Natural products-- Spectra.
Nuclear magnetic resonance.
Organic chemistry.
Organic compounds-- Spectra.
SCIENCE-- Chemistry-- Organic.
Scientific equipment, experiments & techniques.
(SUBJECT CATEGORY (Provisional
PDN
PNN
SCI-- 013040
DEWEY DECIMAL CLASSIFICATION
Number
547
.
046
Edition
23
LIBRARY OF CONGRESS CLASSIFICATION
Class number
QC462
.
5
PERSONAL NAME - PRIMARY RESPONSIBILITY
Burns, Darcy C.
PERSONAL NAME - ALTERNATIVE RESPONSIBILITY
Reynolds, William F.,1937-
ORIGINATING SOURCE
Date of Transaction
20200823053532.0
Cataloguing Rules (Descriptive Conventions))
pn
ELECTRONIC LOCATION AND ACCESS
Electronic name
مطالعه متن کتاب [Book]
Y
