عنوان

Microwave assisted organic synthesis

(Number (ISBN

0849323711

(Number (ISBN

1280764511

(Number (ISBN

1405115602

(Number (ISBN

1405168447

(Number (ISBN

1444305549

(Number (ISBN

1601190697

(Number (ISBN

9780849323713

(Number (ISBN

9781280764516

(Number (ISBN

9781405115605

(Number (ISBN

9781405168441

(Number (ISBN

9781444305548

(Number (ISBN

9781601190697

Number

b620842

Title Proper

Microwave assisted organic synthesis

General Material Designation

[Book]

First Statement of Responsibility

edited by Jason P. Tierney, Pelle Lidström.

Place of Publication, Distribution, etc.

Oxford, UK

Name of Publisher, Distributor, etc.

CRC Press

Date of Publication, Distribution, etc.

©2005.

Specific Material Designation and Extent of Item

(xii, 280 pages) : illustrations, portrait

Text of Note

Cover --; Contents --; Preface --; 1 Theoretical aspects of microwave dielectric heating --; 146;146; Introduction --; 146;246; Theoretical basis of dielectric heating --; 146;346; Dielectric properties of solids --; 146;446; Comparison of microwave and conventional heating --; 146;546; Acknowledgement --; 146;646; References --; 2 Microwave45;accelerated metal catalysis58;organic transformations at warp speed --; 246;146; Introduction --; 246;246; Stille couplings --; 246;346; Suzuki couplings --; 246;446; Negishi couplings --; 246;546; Heck couplings --; 246;646; Cyanation and Sonogashira reactions --; 246;746; Carbon8211;heteroatomcoupling reactions --; 246;846; Asymmetric molybdenum45;catalysed allylic alkylations --; 246;946; Carbonylative couplings --; 246;1046; Outlook --; 246;1146; Acknowledgement --; 246;1246; References --; 3 Heterocyclic chemistry using microwave45;assisted approaches --; 346;146; Introduction --; 346;246; Five45;membered systems with one heteroatom --; 346;346; Five45;membered systems with two heteroatoms --; 346;446; Five45;membered ring systems with more than two heteroatoms --; 346;546; Six45;membered heterocycles containing one heteroatom --; 346;646; Six45;membered heterocycles containing at least two heteroatoms --; 346;746; Seven45;membered heterocycles containing at least two heteroatoms58; 144;4 and 144;545;benzodiazepines --; 346;846; Polycyclic heterocycles --; 346;946; Conclusion --; 346;1046; References --; 4 Microwave45;assisted reductions --; 446;146; Introduction --; 446;246; Reduction of carbon8211;carbonmultiple bonds --; 446;346; Reduction of carbonyl groups --; 446;446; Reduction of nitrogen functional groups --; 446;546; Hydrodehalogenation --; 446;646; Conclusions --; 446;746; References --; 5 Speed and efficiency in the production of diverse structures58; microwave45;assisted multi45;component reactions --; 546;146; Background --; 546;246; Multi45;component reactions --; 546;346; Versatile reagents inmulti45;component reactions --; 546;446; Miscellaneous products --; 546;546; Summary --; 546;646; References --; 6 Integrating microwave45;assisted synthesis and solid45;supported reagents --; 646;146; Introduction --; 646;246; Microwave heating of reactions --; 646;346; Microwave reactions with polymer45;supported reagents --; 646;446; Conclusion --; 646;546; References --; 7 Microwave45;assisted solid45;phase synthesis --; 746;146; Combinatorial chemistry and solid45;phase organic synthesis --; 746;246; Microwave chemistry and solid45;phase organic synthesis --; 746;346; Literature survey --; 746;446; Other types of supports --; 746;546; Conclusion --; 746;646; References --; 8 Timesavings associated with microwave45;assisted synthesis58;a quantitative approach --; 846;146; Introduction --; 846;246; Timesavings associated with microwave45;assisted synthesis --; 846;346; Acceleration of combinatorial library design and development stages --; 846;446; New advances in microwave technology --; 846;546; References --; 9 Scale45;up of microwave45;assisted organic synthesis --; 946;146; Introduction --; 946;246; Mechanisms and effects of microwave heating --; 946;346; Approaches to microwave45;assisted organic chemistry --; 946;446; Safety.

Text of Note

The first reports on the application of microwaves in organic synthesis date back to 1986, but it was not until the recent introduction of specifically designed and constructed equipment, which countered the safety and reproducibility concerns, that synthetic application of microwaves has become established as a laboratory technique. Microwave assisted synthesis is now being adopted in many industrial and academic laboratories to take advantage of the novel chemistry that can be carried out using a variety of organic reaction types. This book demonstrates the underlying principles of microwave.

Composés organiques -- Synthèse.

Microwave heating.

Organic compounds -- Synthesis.

Class number

Book number

edited by Jason P. Tierney, Pelle Lidström.

Jason P Tierney

Pelle Lidström

Electronic name

[Book]

Y