عنوان

Small-scale synthesis of laboratory reagents with reaction modeling

شابک

9781439813126 (hardback)

کد کشور

IR

شماره

E-8185

زبان متن نوشتاري يا گفتاري و مانند آن

انگلیسی

کشور محل نشر

IR

عنوان اصلي

Small-scale synthesis of laboratory reagents with reaction modeling

نام عام مواد

[Book]

نام نخستين پديدآور

/ Leonid Lerner

محل نشرو پخش و غیره

Boca Raton, FL

نام ناشر، پخش کننده و غيره

: CRC Press,

تاریخ نشرو بخش و غیره

, c2011.

نام خاص و کميت اثر

xv, 217 p., [12] p. of plates

ساير جزييات

: ill. (some col.)

ابعاد

; 24 cm.

متن يادداشت

Print - Electronic

متن يادداشت

Includes bibliographical references and index.

متن يادداشت

"When working in a small chemical laboratory attached to a non-chemistry specific project one is frequently asked to solve problems which occur in the main project. Usually one can think of several solutions and experimental testing is required to choose between the different approaches, or indeed to find an approach that works. These often require the use of small amounts of chemicals which the laboratory does not stock. Obtaining these chemicals from commercial suppliers in a suitable timeframe sometimes poses problems. This is particularly the case in isolated regions such as Australasia, when the supplier has no local stocks of hazardous substances and they have to be brought in from overseas, something which can introduce delays from several weeks to six months or more. Since there is no certainty that the substance whose acquisition is introducing the delay will form part of the ultimate solution, this delay is particularly objectionable. The primary aim of this book is therefore to provide reliable laboratory syntheses of the most common reagents whose acquisition can introduce delays due to their hazardous nature. It is apparent that there is little point in replacing delays in reagent purchase with uncertainties in their synthesis, hence the preparations presented in this book were chosen with the following criteria in mind: short duration, availability of apparatus, high yield, and high purity of the product. It was also considered necessary for the syntheses to be described in greater detail than is normally provided in the literature, since I have frequently found that omission of apparently small details can subsequently waste much time"--Provided by publisher.

متن يادداشت

"The in-lab preparation of some chemical reagents provides a number of advantages over purchasing commercially-prepared samples. This volume contains a detailed description of methods for the rapid and reliable synthesis of many useful reagants that are otherwise difficult to obtain. It provides spectroscopic analyses of products, presents the thermodynamic/kinetic data of reactions, and offers a thorough analysis of the purity of the final products. Enhanced by useful diagrams and photographs, this text is a valuable reference for researchers in small or remote laboratories"--Provided by publisher.

موضوع مستند نشده

Chemical tests and reagents--Synthesis

شماره

شماره رده

نشانه اثر

مستند نام اشخاص تاييد نشده

Lerner, Leonid

کشور

ایران

نام ميزبان

Small-scale synthesis of laboratory reagents with reaction modeling/

شماره دسترسي

عادی

اطلاعات مختصر

عادی

نام الکترونيکي

E-8185.pdf

بيت در ثانيه

0

ارتباط براي تسهيلات دسترسي

ایمانی

نوع فرمت الکترونيکي

متن

اندازه فايل

0

شماره کنترل رکورد

E-8185

يادداشت عمومي

انگلیسی

وضعیت فهرست نویسی

old catalog

فرمت انتشار

pe

نوع ماده

BL

پیشوند ISBD اعمال شده است

1

سطح دسترسي

a

تكميل شده

Y