1: Solid Phase Microextraction in Perspective -- 2: Theory of Solid Phase Microextraction -- 3: Development of SPME Devices and Coatings -- 4: SPME Commercial Devices and Fiber Coatings -- 5: Automated SPME Systems -- 6: Calibration -- 7: Solid Phase Microextraction Method Development -- 8: SPME and Environmental Analysis -- 9: Application of Solid Phase Microextraction in Food and Fragrance Analysis -- 01: Drug Analysis by SPME -- 11: Ligand-Receptor Binding and Determination of Free Concentrations -- 21: In Vivo Sampling with Solid Phase Microextraction -- 31: Solid Phase Microextraction Protocols